MULTIPLANT / AUTOPLANT PRECIP: (Mixed) Oxides by pH-Controlled Precipitation, Ion Exchange and Sol-Gel Process

The leading technology in overhead gravimetric dispensing / dosing (patented) combined with our reactor and process excellence, and our user-friendly software, allow you to standardize and accelerate your (mixed) oxide synthesis workflows (precipitation, sol-gel, ion exchange).

Example Customer testimonial

Using Chemspeed’s AUTOPLANT we have been able to test a lot of ideas for making new aluminas in a small amount of time.

Key Advantages:

  • Decrease in cost per experiment up to 90+ %.
  • Increase in productivity by a factor of 10+.
  • Up to 36 experiments per run on an autoplant, up to 6 experiments per run on a multiplant.
  • Independent control of all process parameters in each reactor with PAT like PSD, pH.
  • Independent and precise temperature and stirring control in each reactor.
  • Up to 8 independent liquid feeds per reactor.
  • pH measurement and control (e.g. swingin pH control via acid and base).
  • Vessel-to-vessel transfer for multistep processes.
  • Gravimetric solid and viscous liquid dispensing.
  • 4-Needle Head for volumetric liquid handling and sampling.
  • Feeding and sampling under reaction conditions.
  • Cleaning in place (e.g. automated cleaning, inserts).
  • Dispensed amount, stirrer speed, temperature, pressure, time…, and other data are stored in a read only log file.
  • Easy access to data with a convenient interface to pull results into Excel or virtually any other software.
  • Interface to DOE..

Enhance your Efficiency and Productivity with our Workflow Solutions!

MULTIPLANT AUTOPLANT PRECIP workflow

Assembly of a process research reactor with our unique screwless and self-sealing design up to 100 bar

Assembly of a process research reactor

Technical Details

Chemspeed’s MULTIPLANT/ AUTOPLANT PRECIP deck modularity allows the user to execute and perform a variety of workflows in a fully or semi-automated fashion.

New or better, high-quality (mixed) oxides require accurate control of manyre action parameters, therefore automated workflow solutions are key to accelerate their development.

Reaction preparation

  • Interface to DOE.
  • Gravimetric overhead dispensing of solids powders, and extrudates directly into the reactor.
  • Metal salt solution preparation.
  • Addition of liquid reagents and solutions.

Synthesis

  • Precise liquid and slurry feed with pH-control (acid, base).
  • Excellent mixing for slurries with e.g. 50+ % solid content.
  • Versatile stirring and temperature profiles.
  • Accurate and defined heating programs (+/- 0.1 °C)
      – Standard range: from -20 to 250 °C (Optional extension to -50 °C or 350 °C).
  • Pressure up to 100 bar for e.g. precipitations under superheated conditions.
  • Vessel-to-vessel transfer for multistep processes.
  • Online data visualization.
  • Logging of all reaction parameters.
Work-up

  • Filtration, washing.
  • Centrifugation.
  • Drying.

Post reaction treatment

  • Calcination and desiccation.
  • Compaction, crushing, sieving.

Analytics

  • Powder diffractometer.
  • Electron microscopy.
  • Parallel BET.
  • DSC and TGA.
  • Mercury porosimetry.
Reactor for crystallization development

Process development workstation for 6 X 100 mL, 3 X 250 mL, 3 X 1’000 mL

The cutting edge Process Development Workstation Technology allows scientists to truly mimic the final industrial production process and provides all the flexibility to optimize integrated reaction sequences, even if a complex configuration of reactors and feed vessels required.

Glass, stainless steel, (PEEK, PTFE or glass inserts available), Hastelloy
Materials of choice: glass, stainless steel (PEEK, PTFE or glass inserts available), Hastelloy, others on request

Process reactor assembly, individually controlled tank reactors (reactor volumes 100, 250, 1’000 mL) with precise, continuous feeds.

  • Flexible and precise continuous feeds, down to 10 μL / min.
  • Up to 8 continuous liquid, liquefied gas and / or gas feeds per reactor and additional unlimited overhead access.
  • Accurate and reproducible temperature control, 0.1 °C.
  • Pressure up to 100 bar over the entire temperature range up to 250 °C with corresponding safety installations.
  • Parallel high-performance calorimetry data.
  • Viscosity data.

Exchangeable stirrer designs (anchor, twisted blade, gas entrainment stirrers

Easily exchangeable stirrer designs (anchor, twisted blade, gas entrainment stirrers…). Powerful mixing for viscosities up to 80 Pa.s at 300 rpm and 30 Pa.s at 900 rpm with an anchor stirrer.

Please visit us at:


AOCS Annual Meeting & Industry Showcases
Orlando, USA // 30 April – 3 May 2017
2017 NYSCC Suppliers' Day
New York, USA // 2 – 3 May 2017
10th Annual Global Discovery to Development Innovation Forum (GDDIF)
London, UK // 24 – 25 May 2017
NAM25
Denver, USA // 4 – 9 June 2017

Headquarters

Chemspeed Technologies AG
Wölferstrasse 8
4414 Füllinsdorf
Switzerland
Phone: +41 (0) 61 816 95 00
Fax: +41 (0) 61 816 95 09
chemspeed@chemspeed.com

Mailing list

We send out regular updates about what we are up to. If you'd like to receive these straight to your mailbox, please enter your email address below.

Follow us

google_pluslinkedinyoutube
Send