High output polyolefin and rubber synthesis, optimization, scale-up

MULTIPLANT / AUTOPLANT POSY

Quality by design driven, scalable olefin polymerization, incl. reaction prep, synthesis, work-up, analysis.

Two blue chemspeed robotic platforms in metal sitting in a white hallway

Overview

Chemspeed's solution

The leading technology in overhead gravimetric dispensing / dosing (patented) combined with our quality by desisng reactor technology as well as process excellence and user-friendly software enable you to accelerate, standardize and digitize your polyolefin and rubber synthesis / optimization / scale-up workflows:

solution-phase
slurry-phase
bulk-phase
gas-phase
multi-stage
polymerizations.

Each reactor with its own set of conditions - individually controlled tank reactors (reactor volumes 100, 240, 1’000 mL total volume) with precise, continuous feeds.

Two Chemspeed Swing platforms with raised cantelever doors housing multiple analytic and mixing tools for a laboratory

Workflow

Example workflow

The interactive workflow panel below showcases example workflows for this solution. Each Chemspeed tool or FLEX module performs a set of specific actions, as in any manual lab workflow, and an almost limitless arrangement of these tools is possible.

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MULTIPLANT / AUTOPLANT POSY

Benefits

Powerful advantages

Up to 36 olefin polymerizations per run on an AUTOPLANT, up to 6 per run on a MULTIPLANT.
Integration with / in MBrown glove-box.
Independent control of all process parameters in each reactor with PAT like NIR, PSD, GC(MS).
Independent and precise temperature and stirring control in each reactor.
Up to 8 independent gas, liquefied gas and liquid feeds per reactor.
Gravimetric solid and viscous liquid dispensing.
4-Needle Head for volumetric liquid handling and sampling.
Feeding and sampling under reaction conditions.
Cleaning in place (e.g. automated cleaning, inserts).
Dispensed amount, stirrer speed, temperature, pressure, time, ... and other data are stored in a read only log file.
AUTOSUITE software - drag & drop experimentation with easy interface to data analysis.
Interface for e.g. DOE, ML, AI, LIMS, ELN, ERP integration.

Software

AUTOSUITE

Chemspeed’s AUTOSUITE software packages execute and control all modules in every solution. They control all Chemspeed robotic platforms and any other integrated 3^rd-party software and hardware.

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Chemspeed AutoSuite Software laptop screen