example solution
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High output polyolefin / rubber catalyst synthesis, work-up, analysis

MULTIPLANT / AUTOPLANT POSYCAT
Automated, quality assured, scalable polyolefin and rubber catalyst synthesis.
Two blue chemspeed robotic platforms in metal sitting in a white hallway
Overview

Chemspeed's solution

The leading technology in overhead gravimetric dispensing / dosing (patented) combined with our quality by design reactor and process excellence and user-friendly software enable you to accelerate, standardize and digitize your ligand synthesis & scale up, organometallic synthesis & scale-up (single-site), donor synthesis & scale-up, Ziegler-Natta (ZN) catalyst synthesis workflows (reaction preparation, synthesis, work-up, analysis by online NIR & PSD). 

Workflow

Example workflows

The interactive workflow panel below showcases example workflows for this solution. Each Chemspeed tool or module performs a set of specific actions, as in any manual lab workflow, and an almost limitless arrangement of these tools is possible.

MULTIPLANT / AUTOPLANT POSYCAT - Multi-site (Ziegler-Natta) catalyst synthesis

Details
💡 Click on a workflow node to see more details in this details panel.

MULTIPLANT / AUTOPLANT POSYCAT - Single site ligand and catalyst synthesis

Details
💡 Click on a workflow node to see more details in this details panel.
Benefits

Powerful advantages

Each reactor with its own set of conditions - individually controlled tank reactors (reactor volumes 100, 240, 1’000 mL total volume) with precise, continuous feeds:

  • Up to 36 scalable Ziegler-Natta and / or single site catalyst syntheses per run on an AUTOPLANT, up to 6 catalyst syntheses per run on a MULTIPLANT.
  • Integration with / in MBraun glove-box.
  • Independent control of all process parameters in each reactor with PAT like NIR, PSD.
  • Independent, precise temperature and stirring control in each reactor.
  • Up to 8 independent liquid feeds per reactor.
  • Gravimetric solid and viscous liquid dispensing.
  • 4-Needle Head for volumetric liquid handling and sampling.
  • Feeding and sampling under reaction conditions.
  • Cleaning in place (e.g. automated cleaning, inserts).
  • Dispensed amount, stirrer speed, temperature, pressure, time, ... and other data are stored in a read only log file.
  • Easy access to data with a convenient interface to pull results into Excel or virtually any other software.
  • Interface to DoE.
Software

AUTOSUITE

Chemspeed’s AUTOSUITE software packages execute and control all modules in every solution. They control all Chemspeed robotic platforms and any other integrated 3rd-party software and hardware.

Explore AUTOSUITE
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Automate and digitalize your laboratory with Chemspeed.